[Illustration: FIG. 30.—APPARATUS USED FOR OBTAINING HIGH DEGREES OF EXHAUSTION.]
The apparatus is illustrated in a drawing shown in Fig. 30. S represents a Sprengel pump, which has been specially constructed to better suit the work required. The stop-cock which is usually employed has been omitted, and instead of it a hollow stopper s has been fitted in the neck of the reservoir R. This stopper has a small hole h, through which the mercury descends; the size of the outlet o being properly determined with respect to the section of the fall tube t, which is sealed to the reservoir instead of being connected to it in the usual manner. This arrangement overcomes the imperfections and troubles which often arise from the use of the stopcock on the reservoir and the connection of the latter with the fall tube.
The pump is connected through a U-shaped tube t to a very large reservoir R_1. Especial care was taken in fitting the grinding surfaces of the stoppers p and p_1, and both of these and the mercury caps above them were made exceptionally long. After the U-shaped tube was fitted and put in place, it was heated, so as to soften and take off the strain resulting from imperfect fitting. The U-shaped tube was provided with a stopcock C, and two ground connections g and g_1—one for a small bulb b, usually containing caustic potash, and the other for the receiver r, to be exhausted.
The reservoir R_1 was connected by means of a rubber tube to a slightly larger reservoir R_2, each of the two reservoirs being provided with a stopcock C_1 and C_2, respectively. The reservoir R_2 could be raised and lowered by a wheel and rack, and the range of its motion was so determined that when it was filled with mercury and the stopcock C_2 closed, so as to form a Torricellian vacuum in it when raised, it could be lifted so high that the mercury in reservoir R_1 would stand a little above stopcock C_1; and when this stopcock was closed and the reservoir R_2 descended, so as to form a Torricellian vacuum in reservoir R_1, it could be lowered so far as to completely empty the latter, the mercury filling the reservoir R_2 up to a little above stopcock C_2.
The capacity of the pump and of the connections was taken as small as possible relatively to the volume of reservoir R_1, since, of course, the degree of exhaustion depended upon the ratio of these quantities.
With this apparatus I combined the usual means indicated by former experiments for the production of very high vacua. In most of the experiments it was convenient to use caustic potash. I may venture to say, in regard to its use, that much time is saved and a more perfect action of the pump insured by fusing and boiling the potash as soon as, or even before, the pump settles down. If this course is not followed the sticks, as ordinarily employed, may give moisture off at a certain very slow rate, and the pump may work for many hours without reaching a very high vacuum. The potash was heated either by a spirit lamp or by passing a discharge through it, or by passing a current through a wire contained in it. The advantage in the latter case was that the heating could be more rapidly repeated.


